2R6E
Crystal Form B2
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.98 |
Spacegroup name | H 3 2 |
Unit cell lengths | 199.797, 199.797, 195.036 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 5.019 |
R-factor | 0.39358 |
Rwork | 0.393 |
R-free | 0.39720 |
Structure solution method | SAD |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 5.180 |
High resolution limit [Å] | 5.000 | 5.000 |
Number of reflections | 6233 | |
<I/σ(I)> | 35.9 | 3.5 |
Completeness [%] | 95.8 | 74.5 |
Redundancy | 10.2 | 8.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 2.5M Sodium Chloride, pH 7.0, VAPOR DIFFUSION |