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2R4O

Crystal structure of the long-chain fatty acid transporter FadL mutant delta NPA

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X6A
Synchrotron siteNSLS
BeamlineX6A
Temperature [K]100
Detector technologyCCD
Collection date2005-10-17
DetectorADSC QUANTUM 210
Spacegroup nameP 21 21 21
Unit cell lengths63.050, 146.618, 151.227
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution10.000 - 3.600
R-factor0.243
Rwork0.243
R-free0.31400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1t16
RMSD bond length0.009
RMSD bond angle1.550
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]41.5403.730
High resolution limit [Å]3.6003.600
Rmerge0.2870.593
Number of reflections16885
<I/σ(I)>3.12.2
Completeness [%]98.797
Redundancy4.44
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
15.529535% PEG 2000, 0.05M magnesium acetate, 0.05M cacodylate, pH 5.50, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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