2R44
CRYSTAL STRUCTURE OF A PUTATIVE ATPASE (CHU_0153) FROM CYTOPHAGA HUTCHINSONII ATCC 33406 AT 2.00 A RESOLUTION
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-07-01 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91837, 0.97929, 0.97905 |
Spacegroup name | P 65 |
Unit cell lengths | 120.780, 120.780, 51.170 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.013 - 2.000 |
R-factor | 0.185 |
Rwork | 0.184 |
R-free | 0.21800 |
Structure solution method | MAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.702 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.013 | 29.013 | 2.070 |
High resolution limit [Å] | 2.000 | 4.300 | 2.000 |
Rmerge | 0.049 | 0.027 | 0.519 |
Number of reflections | 28915 | ||
<I/σ(I)> | 13.75 | 32.4 | 2.57 |
Completeness [%] | 99.3 | 98.2 | 95.4 |
Redundancy | 7.35 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.54 | 277 | NANODROP, 0.2M Sodium chloride, 50.0% PEG 200, 0.1M Na/K phosphate pH 6.54, VAPOR DIFFUSION, SITTING DROP, temperature 277K |