2QVV
Porcine Liver Fructose-1,6-bisphosphatase cocrystallized with Fru-2,6-P2 and Zn2+, I(T)-state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-01-29 |
Detector | NOIR-1 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 59.038, 165.709, 79.167 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.330 - 2.030 |
R-factor | 0.201 |
Rwork | 0.200 |
R-free | 0.23400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ID 2QVU |
RMSD bond length | 0.005 |
RMSD bond angle | 1.300 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.080 | 2.130 |
High resolution limit [Å] | 2.030 | 2.030 |
Rmerge | 0.080 | 0.321 |
Total number of observations | 37301 | |
Number of reflections | 51027 | |
<I/σ(I)> | 12 | 3.9 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5.7 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | see citation, pH 7.00, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |