2QP9
Crystal Structure of S.cerevisiae Vps4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Detector technology | CCD |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 86.553, 86.553, 236.061 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.900 |
R-factor | 0.25996 |
Rwork | 0.258 |
R-free | 0.28819 |
Structure solution method | MAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.137 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.063 | 0.606 |
Number of reflections | 12599 | |
<I/σ(I)> | 37.5 | 3.8 |
Completeness [%] | 98.1 | 99.2 |
Redundancy | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 293 | Sodium Acetate, CdSO4, pH 6.5, temperature 293K, VAPOR DIFFUSION |
1 | VAPOR DIFFUSION | 6.5 | 293 | Sodium Acetate, CdSO4, pH 6.5, temperature 293K, VAPOR DIFFUSION |
1 | VAPOR DIFFUSION | 6.5 | 293 | Sodium Acetate, CdSO4, pH 6.5, temperature 293K, VAPOR DIFFUSION |