2QNR
Human septin 2 in complex with GDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-05-05 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.97770 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 164.536, 52.295, 110.944 |
Unit cell angles | 90.00, 132.48, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.600 |
Rwork | 0.234 |
R-free | 0.29300 |
Structure solution method | SAD |
RMSD bond length | 0.015 |
RMSD bond angle | 1.388 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | REFMAC (refmac_5.2.0019) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 20.000 | 22.998 | 2.590 |
High resolution limit [Å] | 2.500 | 5.350 | 2.500 |
Rmerge | 0.057 | 0.033 | 0.435 |
Number of reflections | 22998 | ||
<I/σ(I)> | 17.1 | ||
Completeness [%] | 98.9 | 99.5 | 95.4 |
Redundancy | 7.2 | 7.1 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 291 | PEG 3350, 0.2M Trilithium citrate, 0.1M Bis-Tris, pH 6.5, VAPOR DIFFUSION, temperature 291K |