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2QMZ

Quinone Reductase 2 in Complex with Dopamine

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-BM
Synchrotron siteAPS
Beamline19-BM
Temperature [K]100
Detector technologyCCD
Collection date2005-07-29
DetectorCUSTOM-MADE
Wavelength(s)1
Spacegroup nameP 21 21 21
Unit cell lengths83.442, 106.448, 56.533
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 2.100
Rwork0.193
R-free0.23800
Structure solution methodMOLECULAR REPLACEMENT
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]2.100
Rmerge0.101
Number of reflections28148
<I/σ(I)>15
Completeness [%]93.6
Redundancy6.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7300Ammonium Sulfate (1.2-2 M), pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 300K

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