2Q81
Crystal Structure of the Miz-1 BTB/POZ domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX14.2 |
Synchrotron site | SRS |
Beamline | PX14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-08 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.979 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 65.535, 128.522, 116.038 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 12.000 - 2.100 |
R-factor | 0.184 |
Rwork | 0.181 |
R-free | 0.22900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2nn2 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.179 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MrBUMP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.260 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.052 | 0.300 |
Number of reflections | 28911 | |
<I/σ(I)> | 21.7 | 6.1 |
Completeness [%] | 99.8 | 100 |
Redundancy | 6.1 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | 20% PEG 3350, 20% PEG 400, 200 mM MgCl2, 100 mM HEPES pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |