2Q6O
SalL-Y70T with SAM and Cl
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Detector technology | CCD |
Collection date | 2006-09-01 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1 |
Spacegroup name | P 3 |
Unit cell lengths | 111.530, 111.530, 47.610 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.270 - 2.000 |
R-factor | 0.26869 |
Rwork | 0.266 |
R-free | 0.31298 |
Structure solution method | 2Q6I |
RMSD bond length | 0.021 |
RMSD bond angle | 2.043 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.120 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.156 | 0.256 |
Number of reflections | 44611 | |
<I/σ(I)> | 7.13 | 4.36 |
Redundancy | 3.5 | 3.34 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | 28% PEG3350, 0.3M KCL, 2mM DTT, 0.1 M MOPSO, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 277K |