2PY8
RbcX
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-10-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97947,0.97969,0.97182 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 129.832, 129.832, 92.742 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.500 - 2.450 |
R-factor | 0.211 |
Rwork | 0.209 |
R-free | 0.24900 |
Structure solution method | MAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.137 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.000 | 2.540 |
High resolution limit [Å] | 2.450 | 2.450 |
Rmerge | 0.059 | 0.541 |
Number of reflections | 29666 | |
<I/σ(I)> | 16.7 | |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.7 | 7.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 298 | 30% PEG 400, 0.1M potassium/sodium phosphate, 0.2M lithium sulfate, pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 298 | 30% PEG 400, 0.1M potassium/sodium phosphate, 0.2M lithium sulfate, pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 298 | 30% PEG 400, 0.1M potassium/sodium phosphate, 0.2M lithium sulfate, pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |