2PWU
tRNA guanine transglycosylase in complex with guanine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Collection date | 2007-01-17 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54178 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 90.151, 64.503, 70.769 |
Unit cell angles | 90.00, 92.79, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.770 |
Rwork | 0.200 |
Structure solution method | AB INITIO |
Starting model (for MR) | 1p0b |
RMSD bond length | 0.006 |
RMSD bond angle | 0.023 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELX |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.800 |
High resolution limit [Å] | 1.770 | 1.770 |
Rmerge | 0.035 | 0.389 |
Number of reflections | 34387 | |
<I/σ(I)> | 22 | 2.3 |
Completeness [%] | 94.8 | 0.839 |
Redundancy | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 291 | pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |