2PWJ
Structure of a mitochondrial type II peroxiredoxin from Pisum sativum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR-H |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-02-02 |
Detector | BRUKER PLATINUM 200 |
Spacegroup name | P 1 |
Unit cell lengths | 61.880, 66.400, 77.230 |
Unit cell angles | 102.94, 104.44, 99.07 |
Refinement procedure
Resolution | 14.980 - 2.800 |
R-factor | 0.298 |
Rwork | 0.277 |
R-free | 0.29200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | model generated by EasyPed3D Web Server 1.0 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.900 |
Data reduction software | SAINT |
Data scaling software | SAINT (V7.12A) |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 71.900 | 2.480 | |
High resolution limit [Å] | 2.390 | 5.170 | 2.400 |
Number of reflections | 30073 | ||
<I/σ(I)> | 15.416 | ||
Completeness [%] | 65.8 | ||
Redundancy | 3.08 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 293 | PEG2000, citrate, NaCl, DTT, 2-propanol, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |