2PKC
CRYSTAL STRUCTURE OF CALCIUM-FREE PROTEINASE K AT 1.5 ANGSTROMS RESOLUTION
Experimental procedure
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 68.270, 68.270, 108.080 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 1.500 |
| R-factor | 0.201 |
| Refinement software | TNT |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 * |
| High resolution limit [Å] | 1.500 * |
| Rmerge | 0.147 * |
| Number of reflections | 33854 * |
| Completeness [%] | 78.0 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 6 (%(w/v)) | |
| 2 | 1 | drop | Tris-HCl | 50 (mM) | |
| 3 | 1 | drop | sodium-EDTA | 300 (mM) | |
| 4 | 1 | drop | 0.02 (%) | ||
| 5 | 1 | reservoir | 0.75 (M) |
