2PIO
Androgen receptor LBD with small molecule
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-03-09 |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.616, 66.015, 70.547 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 - 2.030 |
Rwork | 0.245 |
R-free | 0.28680 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | ELVES |
Data scaling software | SCALA |
Phasing software | CNS |
Refinement software | ELVES |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | |
High resolution limit [Å] | 2.030 | 2.030 |
Rmerge | 0.063 | 0.063 |
Number of reflections | 17047 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | VAPOR DIFFUSION, SITTING DROP, temperature 298K |