2PII

PII, GLNB PRODUCT

Experimental procedure

Spacegroup name	P 63
Unit cell lengths	61.600, 61.600, 56.300
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 1.900
R-factor	0.132
Rwork	0.132
RMSD bond length	0.017
RMSD bond angle	1.980
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	1.900 *
Rmerge	0.071 *
Total number of observations	45387 *
Number of reflections	11079

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7 *	4 *	Vasudevan, S.G., (1994) FEBS Lett., 337, 255. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	8 (mg/ml)
2	1	drop	phosphate	1 (M)
3	1	reservoir	phosphate	2 (M)