Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.600, 72.800, 115.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.500 - 2.800 |
R-factor | 0.154 |
Rwork | 0.154 |
R-free | 0.29500 * |
RMSD bond length | 0.013 |
RMSD bond angle | 1.900 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.800 * |
Rmerge | 0.087 * |
Total number of observations | 44042 * |
Number of reflections | 13290 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | pHb | 0.5 (mM) | solubilized in 10 mM ammonium phosphate |
2 | 1 | reservoir | 2.8-2.9 (M) | ||
3 | 1 | reservoir | 2.8-2.9 (M) |