2PGA

X-ray Structure of the Uridine Phosphorylase From SALMONELLA TYPHIMURIUM in Complex with Inhibitor and Phosphate and Potassium Ion at 1.74 A Resolution

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE X13
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	X13
Detector technology	CCD
Collection date	2004-12-21
Detector	MAR CCD 165 mm
Spacegroup name	P 21 21 21
Unit cell lengths	88.790, 124.070, 134.110
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 1.740
Rwork	0.181
R-free	0.20980
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	28.090
High resolution limit [Å]	1.720
Number of reflections	145178

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		297	VAPOR DIFFUSION, HANGING DROP, temperature 297K