Experimental procedure
| Detector technology | AREA DETECTOR |
| Collection date | 1990 |
| Detector | SIEMENS |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 129.300, 126.900, 76.900 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.250 |
| R-factor | 0.164 * |
| Rwork | 0.164 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.038 |
| Data reduction software | XENGEN |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 9999.000 * | |
| High resolution limit [Å] | 2.250 | 2.250 * |
| Rmerge | 0.079 | 0.150 * |
| Total number of observations | 173209 * | |
| Number of reflections | 50764 | 4508 * |
| Completeness [%] | 88.0 | 42.3 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | protein | 0.6 (%) | |
| 2 | 1 | 1 | sodium phosphate | 0.05 (M) | |
| 3 | 1 | 1 | PEG6000 | 12 (%(w/v)) |
