2PCP
ANTIBODY FAB COMPLEXED WITH PHENCYCLIDINE
Experimental procedure
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1997-08 |
Detector | MACSCIENCE |
Spacegroup name | P 1 |
Unit cell lengths | 53.460, 67.720, 68.040 |
Unit cell angles | 62.11, 84.66, 83.17 |
Refinement procedure
Resolution | 6.000 - 2.200 |
R-factor | 0.199 * |
Rwork | 0.196 |
R-free | 0.28600 * |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4FAB AND 1GIG |
RMSD bond length | 0.015 * |
RMSD bond angle | 2.400 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 2.400 | |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.091 | 0.221 |
Total number of observations | 69236 * | |
Number of reflections | 33694 | |
<I/σ(I)> | 9.8 | 3.7 |
Completeness [%] | 79.3 | 63.5 |
Redundancy | 2.1 | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4.6 | pH 4.6 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 15 (mg/ml) | |
2 | 1 | reservoir | ammonium sulfate | 2.2 (M) | |
3 | 1 | reservoir | sodium acetate | 0.1 (M) |