2P4F
Crystal Structure of Atp11 functional domain from Candida Glabrata
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-01-01 |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 0.97625 |
Spacegroup name | I 41 |
Unit cell lengths | 63.187, 63.187, 153.577 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.400 |
R-factor | 0.1449 |
Rwork | 0.145 |
R-free | 0.18620 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 0.031 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.420 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.058 | 0.476 |
Number of reflections | 47858 | |
<I/σ(I)> | 16.1 | 1.59 |
Completeness [%] | 81.2 | 15.3 |
Redundancy | 10.3 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | PEG 400, MES, Acetate, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | PEG 400, MES, Acetate, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K |