2P3V
Thermotoga maritima IMPase TM1415
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2004-11-27 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 83.814, 97.939, 122.156 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.000 - 2.400 |
R-factor | 0.18 |
Rwork | 0.178 |
R-free | 0.26300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Model built from human AF MJ IMPases |
RMSD bond length | 0.007 |
RMSD bond angle | 1.250 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.063 | 0.550 |
Number of reflections | 36088 | |
<I/σ(I)> | 10.1 | 1.1 |
Completeness [%] | 98.0 | 96 |
Redundancy | 2.5 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293 | 15% PEG 400, 0.2M tartrate, 0.2M ammonium sulfate, 50mM citrate, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 293K |