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2OY0

Crystal structure of the West Nile virus methyltransferase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X4A
Synchrotron siteNSLS
BeamlineX4A
Temperature [K]100
Detector technologyCCD
Collection date2004-02-13
DetectorADSC QUANTUM 4
Wavelength(s)1.00925
Spacegroup nameP 1
Unit cell lengths39.229, 66.009, 78.761
Unit cell angles112.46, 102.90, 89.80
Refinement procedure
Resolution39.120 - 2.800
R-factor0.259
Rwork0.259
R-free0.33400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1l9k
RMSD bond length0.008
RMSD bond angle1.400
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareAMoRE
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]39.1202.960
High resolution limit [Å]2.8002.800
Rmerge0.1120.214
Number of reflections15957
<I/σ(I)>4.32.5
Completeness [%]0.90.917
Redundancy1.71.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.629813 to 15% PEG4000, 5% isopropanol, 0.1M sodium citrate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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