Experimental procedure
| Detector technology | AREA DETECTOR |
| Collection date | 1996-01 |
| Detector | SIEMENS |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 156.230, 49.040, 42.250 |
| Unit cell angles | 90.00, 98.60, 90.00 |
Refinement procedure
| Resolution | 9.000 - 2.000 * |
| R-factor | 0.186 * |
| RMSD bond length | 0.009 |
| RMSD bond angle | 18.000 * |
| Data reduction software | SAINT |
| Refinement software | TNT |
Data quality characteristics
| Overall | |
| Rmerge | 0.052 |
| Total number of observations | 46251 * |
| Number of reflections | 19026 |
| Completeness [%] | 85.5 |
| Redundancy | 2.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, sitting drop * | 7.4 * | 20 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ammonium salfate | 1.8-1.9 (M) | |
| 2 | 1 | reservoir | sodium phosphate | 30 (mM) |
