Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.6 |
| Synchrotron site | SRS |
| Beamline | PX9.6 |
| Temperature [K] | 123 |
| Detector technology | IMAGE PLATE |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.875 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 109.190, 76.040, 70.280 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.400 |
| R-factor | 0.183 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 0.029 |
| Data reduction software | MOSFLM |
| Data scaling software | XDS |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 17.960 | |
| High resolution limit [Å] | 1.360 | |
| Rmerge | 0.097 | 0.204 * |
| Number of reflections | 109232 | |
| Completeness [%] | 88.3 | 84.2 * |
| Redundancy | 2.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 5.5 | pH 5.5 | |
| 1 | unknown * | 5.5 | pH 5.5 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | PEG4000 | 7-10 (%) | |
| 2 | 1 | reservoir | sodium acetate | 50 (mM) | |
| 3 | 1 | reservoir | uranyl acetate | 1 (mM) |
