2OK6
Crystal structure of aromatic amine dehydrogenase TTQ-formamide adduct oxidized with ferricyanide.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.338, 89.266, 80.494 |
Unit cell angles | 90.00, 90.59, 90.00 |
Refinement procedure
Resolution | 15.000 - 1.450 |
R-factor | 0.16242 |
Rwork | 0.161 |
R-free | 0.19172 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.013 |
RMSD bond angle | 1.542 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.450 |
Number of reflections | 161574 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 292 | PEG 2000 MME, AMMONIUM SULPHATE,SODIUM CACODYLATE, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 292K |