2OJH
The structure of putative TolB from Agrobacterium tumefaciens
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-03 |
Detector | CUSTOM-MADE |
Wavelength(s) | 0.97918, 0.97935 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 144.714, 56.159, 48.332 |
Unit cell angles | 90.00, 107.95, 90.00 |
Refinement procedure
Resolution | 35.500 - 1.850 |
R-factor | 0.17224 |
Rwork | 0.170 |
R-free | 0.21594 |
Structure solution method | MAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.462 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.500 | 1.890 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 29685 | |
<I/σ(I)> | 9.7 | 3.4 |
Completeness [%] | 93.8 | 70.1 |
Redundancy | 6.5 | 5.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1M Sodium cacodylate pH 6.5, 0.2M Magnesium acetate, 20% PEG 8000, VAPOR DIFFUSION, HANGING DROP, temperature 293K |