2OE4
High Pressure Psuedo Wild Type T4 Lysozyme
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2004-11-15 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 60.741, 60.741, 96.028 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 52.630 - 2.100 |
R-factor | 0.164 |
Rwork | 0.161 |
R-free | 0.22200 |
Structure solution method | ISOMORPHOUS REPLACEMENT |
Starting model (for MR) | 1l63 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.446 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.070 | 0.202 |
Number of reflections | 12182 | |
<I/σ(I)> | 17.9 | |
Completeness [%] | 96.8 | 93.7 |
Redundancy | 6.7 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.1 | 293 | ~2.0 M NA/K PHOSPHATES, 50 MM BETA-MERCAPTOETHANOL, pH 7.1, VAPOR DIFFUSION, HANGING DROP, temperature 293K |