2OB1
ppm1 with 1,8-ANS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-05-05 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.81 |
Spacegroup name | P 65 |
Unit cell lengths | 110.620, 110.620, 161.940 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 83.040 - 1.900 |
R-factor | 0.184 |
Rwork | 0.182 |
R-free | 0.22400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1rjd |
RMSD bond length | 0.015 |
RMSD bond angle | 1.524 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | AMoRE |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 83.045 | 1.950 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 88060 | |
Completeness [%] | 100.0 | 95.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 300 | 15% PEG 8000, 0.2M ammonium sulfate, 0.1M MES, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 300K |