2OA2
Crystal structure of BH2720 (10175341) from Bacillus halodurans at 1.41 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-19 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91837, 0.97971, 0.97925 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 68.610, 68.610, 60.106 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.507 - 1.410 |
R-factor | 0.166 |
Rwork | 0.165 |
R-free | 0.18900 |
Structure solution method | MAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.709 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.507 | 1.460 | |
High resolution limit [Å] | 1.410 | 2.410 | 1.410 |
Rmerge | 0.051 | 0.051 | 0.457 |
Number of reflections | 26400 | ||
<I/σ(I)> | 21.48 | 42.8 | 2.6 |
Completeness [%] | 91.5 | 99.9 | 59.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP, NANODROP | 6 | 277 | 10.0% MPD, 0.1M MES pH 6.0, VAPOR DIFFUSION, SITTING DROP, NANODROP, temperature 277K |