2O8G
Rat pp1c gamma complexed with mouse inhibitor-2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-10 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 96.267, 103.234, 149.992 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.800 - 2.500 |
R-factor | 0.197 |
Rwork | 0.194 |
R-free | 0.23500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2o8a |
RMSD bond length | 0.010 |
RMSD bond angle | 1.184 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | REFMAC |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.090 | 0.610 |
Number of reflections | 52166 | |
<I/σ(I)> | 8.7 | 1.9 |
Completeness [%] | 99.5 | 95.9 |
Redundancy | 5.4 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.6 | 288 | 100 mM Tris-HCL, 150 mM Sodium Citrate, 20% (w/v) PEG 3350, pH 8.6, VAPOR DIFFUSION, SITTING DROP, temperature 288K |