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2O6F

Structure of metal- free rTp34 from Treponema pallidum

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-BM
Synchrotron siteAPS
Beamline19-BM
Temperature [K]100
Detector technologyCCD
Collection date2006-07-14
DetectorCUSTOM-MADE
Wavelength(s)0.97899
Spacegroup nameP 21 21 21
Unit cell lengths34.251, 66.034, 151.019
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution26.030 - 1.630
R-factor0.19
Rwork0.189
R-free0.21900
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)native protein
RMSD bond length0.015
RMSD bond angle1.893
Data reduction softwareHKL-3000
Data scaling softwareHKL-3000
Phasing softwareCNS
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]26.0301.660
High resolution limit [Å]1.6301.630
Number of reflections41967
<I/σ(I)>322.2
Completeness [%]95.394.1
Redundancy4.13.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP92932.4 M Ammonium sulfate, 0.1 M Bicine, pH 9.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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