2O5S
Cobalt horse heart myoglobin, nitrite modified
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2006-05-10 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.54178 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 35.168, 28.680, 63.356 |
| Unit cell angles | 90.00, 106.09, 90.00 |
Refinement procedure
| Resolution | 26.580 - 1.600 |
| R-factor | 0.17624 |
| Rwork | 0.174 |
| R-free | 0.21524 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 2.280 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 26.580 |
| High resolution limit [Å] | 1.600 |
| Rmerge | 0.044 |
| Number of reflections | 15758 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 296 | Ammonium sulfate, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 296K |
