2O2W
Extending powder diffraction to proteins: structure solution of the second SH3 domain from ponsin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID13 |
| Synchrotron site | ESRF |
| Beamline | ID13 |
| Temperature [K] | 295 |
| Detector technology | SCINTILLATOR |
| Collection date | 2006-03-13 |
| Detector | NINE AVALANCHE PHOTODIODE (APD) DETECTORS |
| Wavelength(s) | 0.8012034, 1.241209, 1.242481 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 24.704, 36.426, 72.099 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - ? |
| Data scaling software | ID31SUM |
| Phasing software | MOLREP |
| Refinement software | GSAS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 36.000 |
| High resolution limit [Å] | 2.270 |
| Number of reflections | 32259 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | SMALL TUBES | 7.5 | 292 | TRIS/HCL 0.025M, NaCl 0.9M, pH 7.5, SMALL TUBES, temperature 292K |
