Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2006-07-12 |
| Detector | RIGAKU |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.187, 63.765, 64.742 |
| Unit cell angles | 90.00, 91.81, 90.00 |
Refinement procedure
| Resolution | 45.410 - 1.800 |
| R-factor | 0.189 |
| Rwork | 0.186 |
| R-free | 0.23700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.476 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.410 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 33633 | |
| Completeness [%] | 89.7 | 49.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 300 | 0.1M BICINE pH 9.0, 27% PEG3350, 0.2M MgCl2, PH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 300K |
