2NYC
Crystal structure of the Bateman2 domain of yeast Snf4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Detector technology | CCD |
Collection date | 2005-06-22 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 64.184, 64.184, 61.141 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.400 - 1.900 |
R-factor | 0.20623 |
Rwork | 0.205 |
R-free | 0.23802 |
Structure solution method | SAD |
RMSD bond length | 0.015 |
RMSD bond angle | 1.545 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.900 |
Number of reflections | 11833 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.5 | 294 | 30% (w/v) PEG4000 and 200 mM (NH4)Acetate, pH 4.5, VAPOR DIFFUSION, temperature 294K |