2NNU
Crystal Structure of the Papillomavirus DNA Tethering Complex E2:Brd4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Detector technology | CCD |
Collection date | 2005-10-25 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.1159 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 52.892, 94.589, 119.691 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.590 |
R-factor | 0.20133 |
Rwork | 0.200 |
R-free | 0.23331 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dto |
RMSD bond length | 0.014 |
RMSD bond angle | 1.427 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.650 |
High resolution limit [Å] | 1.590 | 1.590 |
Number of reflections | 40019 | |
<I/σ(I)> | 18.6 | 5 |
Completeness [%] | 98.4 | 92.1 |
Redundancy | 3.3 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 277 | 100mM citrate, 1.8-2.0M Na-acetate, 10mM DTT, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 277K |