2N3F

Solution structure of both dsRBDs of DRB4 along with linker (viz. DRB4(1-153))

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D (H)C(CO)NH-TOCSY
11	1	2	3D HCCH-TOCSY
12	1	2	3D HNHA
13	1	7	2D 1H-13C HSQC
14	1	3	2D 1H-13C HSQC
15	1	4	3D 1H-13C NOESY
16	1	5	2D 1H-15N HSQC
17	1	5	2D 1H-1H NOESY
18	1	3	2D 1H-15N HSQC
19	1	6	2D 1H-15N HSQC
2	1	2	3D HNCO
20	1	1	3D 1H-15N NOESY
21	1	2	3D 1H-13C NOESY
3	1	2	3D HN(CA)CO
4	1	2	3D HNCA
5	1	2	3D HN(CO)CA
6	1	2	3D HNCACB
7	1	2	3D HN(COCA)CB
8	1	2	2D 1H-13C HSQC
9	1	2	3D H(CCO)NH-TOCSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7.2	ambient	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	10