2N2F

Solution NMR structure of Dynorphin 1-13 bound to Kappa Opioid Receptor

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III	Bruker Avance III	800
2	Bruker	AVANCE	Bruker Avance	800
3	Bruker	AVANCE III	Bruker Avance III	700
4	Bruker	AVANCE III	Bruker Avance III	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-1H TOCSY
2	1	1	2D 1H-1H NOESY
3	1	1	2D 1H-15N HSQC
4	1	2	2D 1H-13C HSQC
5	1	2	2D HNCACB
6	1	1	15N T1 T2 hetNOE
7	1	2	15N T2

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.1	ambient	280

Conformers

Conformers Calculated Total Number	1000
Conformers Submitted Total Number	10