2N0K

Chemical shift assignments and structure of the alpha-crystallin domain from human, HSPB5

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	800
2	Bruker	AVANCE	Bruker Avance	600
3	Bruker	AVANCE	Bruker Avance	500
4	Bruker	AVANCE	Bruker Avance	900

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D HNCA
11	1	2	3D HN(CO)CA
12	1	2	3D HN(COCA)CB
13	1	4	3D HCCH-TOCSY
14	1	5	3D H(CCO)NH
15	1	5	3D C(CO)NH
2	2	2	2D 1H-15N HSQC
3	1	2	2D 1H-15N HSQC
4	1	1	3D 1H-15N NOESY
5	1	4	2D 1H-13C HSQC aliphatic
6	1	4	2D 1H-13C HSQC aromatic
7	1	2	3D HNCACB
8	1	2	3D HBHA(CO)NH
9	1	2	3D HNCO

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7.5	ambient	295
2	6.5	ambient	295

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	9