2MNW

Solution structure of the P22S mutant of N-terminal CS domain of human Shq1

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	800
2	Bruker	DRX	Bruker DRX	600
3	Bruker	DRX	Bruker DRX	500

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D HCCH-TOCSY
11	1	2	3D HBHA(CO)NH
12	1	3	3D 1H-13C NOESY aliphatic
13	1	2	3D 1H-15N NOESY
14	1	3	3D 1H-13C NOESY aromatic
15	1	1	3D HNHA
16	1	2	3D HCACO
2	1	2	2D 1H-13C HSQC
3	1	2	3D CBCA(CO)NH
4	1	2	3D C(CO)NH
5	1	2	3D HNCO
6	1	2	3D HNCA
7	1	2	3D HNCACB
8	1	2	3D HN(CO)CA
9	1	3	3D HCCH-TOCSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	ambient	298

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20