2MMZ

Solution structure of the apo form of human glutaredoxin 5

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	500
2	Bruker	AVANCE	Bruker Avance	700
3	Bruker	AVANCE	Bruker Avance	800
4	Bruker	AVANCE	Bruker Avance	900

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D HN(CO)CA
11	1	1	3D 1H-15N NOESY
12	1	2	3D 1H-13C NOESY aliphatic
13	1	2	3D HN(CA)CO
2	1	2	2D 1H-13C HSQC
3	1	2	3D HCCH-TOCSY
4	1	1	2D 1H-1H NOESY
5	1	2	3D CBCA(CO)NH
6	1	2	3D HNCO
7	1	2	3D HNCA
8	1	2	3D HNCACB
9	1	2	3D HBHA(CO)NH

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	ambient	298

Conformers

Conformers Calculated Total Number	80
Conformers Submitted Total Number	20