2MJB

Solution nmr structure of ubiquitin refined against dipolar couplings in 4 media

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	500
2	Bruker	AVANCE	Bruker Avance	600
3	Bruker	AVANCE	Bruker Avance	800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N IPAP HSQC
2	1	2	2D 1H-15N IPAP HSQC
3	1	1	2D 1H-15N TROSY HSQC
4	1	2	2D 1H-15N TROSY HSQC
5	1	1	3D TROSY HNCO
6	1	2	3D TROSY HNCO
7	2	3	3D HN(CO)CA 1H-1H decoupled
8	2	4	1H-15N ARTSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6	ambient	308
2	6	ambient	298

Conformers

Conformers Calculated Total Number	20
Conformers Submitted Total Number	20