2MHP
Solution structure of the major factor VIII binding region on von Willebrand factor
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Varian | INOVA | Varian INOVA | 600 |
2 | Bruker | AVANCE III | Bruker Avance III | 500 |
3 | Bruker | AVANCE III | Bruker Avance III | 700 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 3D HNCO |
10 | 1 | 2 | 2D constant-time 1H-13C HSQC |
11 | 1 | 1 | 3D 1H-15N NOESY |
12 | 1 | 4 | 3D 1H-13C NOESY |
13 | 1 | 3 | {1H}15N steady-state NOE |
14 | 1 | 3 | 15N R1rho relaxation |
15 | 1 | 3 | 15N R1 relaxation |
16 | 1 | 5 | 15N R2-CPMG relaxation dispersion |
17 | 1 | 5 | 15N R2-CPMG relaxation dispersion |
18 | 1 | 6 | 2D IPAP-15N HSQC |
19 | 1 | 7 | 2D IPAP-15N HSQC |
2 | 1 | 1 | 3D HNCA |
20 | 1 | 8 | 2D IPAP-15N HSQC |
21 | 1 | 6 | 2D IPAP-E.COSY-15N HSQC |
22 | 1 | 8 | 2D IPAP-E.COSY-15N HSQC |
23 | 1 | 6 | 3D IPAP-HNCO(J-CA) |
24 | 1 | 8 | 3D IPAP-HNCO(J-CA) |
25 | 1 | 6 | 3D HN(CO)CA(J-CB) |
26 | 1 | 8 | 3D HN(CO)CA(J-CB) |
27 | 1 | 6 | 3D IPAP-(HA)CA(CO)NH |
28 | 1 | 8 | 3D IPAP-(HA)CA(CO)NH |
29 | 1 | 1 | 2D 1H-15N HSQC |
3 | 1 | 1 | 3D HN(CO)CA |
30 | 1 | 1 | 2D 1H-13C HSQC |
31 | 1 | 1 | 2D constant-time 1H-13C HSQC |
32 | 1 | 4 | 2D 1H-13C HSQC |
33 | 1 | 4 | 2D constant-time 1H-13C HSQC |
4 | 1 | 1 | 3D HNCACB |
5 | 1 | 1 | 3D 15N HSQC-NOESY-15N HSQC |
6 | 1 | 1 | 3D HN(CACO)NH |
7 | 1 | 1 | 3D (H)CC(CO)NH |
8 | 1 | 1 | 3D H(CCCO)NH |
9 | 1 | 1 | 3D HCCH-TOCSY |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 7.4 | ambient | 298 |
Conformers
Conformers Calculated Total Number | 100 |
Conformers Submitted Total Number | 10 |