2MGJ

HIGH RESOLUTION CRYSTAL STRUCTURES OF FIVE DISTAL HISTIDINE MUTANTS OF SPERM WHALE MYOGLOBIN

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2 Å)

Cell axes91.20091.20045.870
Cell angles90.0090.00120.00
SpacegroupP 6
Resolution limits5.00 - 2.00
the highest resolution shell value -
R-factor0.156
R-work0.15600
RMSD bond length0.018
RMSD bond angle2.359

Data Collection Statistics

Resolution limits - 2.00*
the highest resolution shell value -
Rmerge_l_obs0.085*
Completeness95.1*

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
111protein60 (mg/ml)
211ammonium sulfate2.4 (M)
311Tris-HCl15 (mM)
411EDTA0.75 (mM)
Annotated Information is extracted from Literature Info*