2MGF

HIGH RESOLUTION CRYSTAL STRUCTURES OF FIVE DISTAL HISTIDINE MUTANTS OF SPERM WHALE MYOGLOBIN

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (1.8 Å)

Cell axes91.20091.20045.870
Cell angles90.0090.00120.00
SpacegroupP 6
Resolution limits5.00 - 1.80
the highest resolution shell value -
R-factor0.152
R-work0.15200
RMSD bond length0.022
RMSD bond angle2.777

Data Collection Statistics

Resolution limits - 1.80*
the highest resolution shell value -
Rmerge_l_obs0.066*
Completeness81.4*

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
111protein60 (mg/ml)
211ammonium sulfate2.4 (M)
311Tris-HCl15 (mM)
411EDTA0.75 (mM)
Annotated Information is extracted from Literature Info*