Experimental procedure
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 6 |
Unit cell lengths | 91.390, 91.390, 45.750 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 5.000 - 1.500 |
R-factor | 0.179 |
Rwork | 0.179 |
RMSD bond length | 0.018 |
RMSD bond angle | 19.500 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 18.200 |
High resolution limit [Å] | 1.500 |
Rmerge | 0.025 |
Number of reflections | 32143 |
Completeness [%] | 91.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * | 9 | 17 * | pH 9. |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 60 (mg/ml) | |
2 | 1 | 1 | ammonium sulfate |