2M8R

Pre-Fusion Solution NMR Structure of Neuronal SNARE Syntaxin 1A

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	800
2	Bruker	AVANCE	Bruker Avance	600
3	Varian	INOVA	Varian INOVA	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D H(CCO)NH
11	1	2	3D C(CO)NH
12	1	2	2D 1H-13C HSQC aromatic
13	1	2	2D 1H-13C HSQC aliphatic
14	1	2	3D 1H-15N NOESY
15	1	2	3D 1H-13C NOESY
16	1	1	3D 1H-15N NOESY
2	1	2	2D 1H-15N HSQC
3	1	1	3D HNCO
4	1	1	3D HNCA
5	1	1	3D HNCACB
6	1	1	3D HN(CO)CA
7	1	2	3D HNHA
8	1	2	3D HCCH-TOCSY
9	1	2	3D HCCH-COSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	5.5	ambient	313

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20