2M83

Solution structure of the carbohydrate binding module of the muscle glycogen-targeting subunit of Protein Phosphatase-1

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	500
2	Bruker	AVANCE	Bruker Avance	800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	3	2D 1H-1H COSY
11	1	1	3D 1H-15N NOESY
12	1	2	3D 1H-13C NOESY
2	1	2	3D HNCACB
3	1	2	3D CBCA(CO)NH
4	1	2	3D HNCA
5	1	2	3D (H)CC(CO)NH
6	1	2	3D HBHA(CO)NH
7	1	2	3D HCCH-TOCSY
8	1	3	2D 1H-1H NOESY
9	1	3	2D 1H-1H TOCSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.5	ambient	298

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	20