2M74
1H, 13C and 15N assignments of the four N-terminal domains of human fibrillin-1
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Home-built | home-built using GE Omega software | home-built home-built using GE Omega software | 750 |
2 | Home-built | home-built using GE Omega software | home-built home-built using GE Omega software | 600 |
3 | Bruker | AVANCE | Bruker Avance | 500 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 2D 1H-15N HSQC |
10 | 1 | 3 | 3D HN(CA)CO |
11 | 1 | 4 | 2D 1H-13C HSQC aliphatic |
12 | 1 | 4 | 3D HCCH-TOCSY |
13 | 1 | 4 | 3D 1H-13C NOESY aliphatic |
14 | 1 | 4 | 2D 1H-13C HSQC aromatic |
15 | 1 | 1 | 3D 1H-15N HSQC-NOESY-HSQC |
16 | 1 | 1 | 2D 1H-15N HMQC-J |
17 | 2 | 5 | 2D 1H-15N IPAP-HSQC |
2 | 1 | 1 | 3D 1H-15N NOESY |
3 | 1 | 1 | 3D 1H-15N TOCSY |
4 | 1 | 2 | 2D 1H-1H TOCSY |
5 | 1 | 2 | 2D DQF-COSY |
6 | 1 | 2 | 2D 1H-1H NOESY |
7 | 1 | 3 | 3D HNCA |
8 | 1 | 3 | 3D (H)CC(CO)NH |
9 | 1 | 3 | 3D HNCO |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 5.4 | 1 | 298 |
2 | 5.4 | 1 | 308 |
Conformers
Conformers Calculated Total Number | 200 |
Conformers Submitted Total Number | 20 |