2M64
1H, 13C and 15N Chemical Shift Assignments for Phl p 5a
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | DMX | Bruker DMX | 500 |
| 2 | Bruker | DMX | Bruker DMX | 600 |
| 3 | Bruker | DMX | Bruker DMX | 900 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 3 | 2D 1H-15N HSQC |
| 2 | 1 | 3 | 3D HNCO |
| 3 | 1 | 3 | 3D HNCACB |
| 4 | 1 | 3 | 3D HBHA(CO)NH |
| 5 | 1 | 1 | 4D HCCH NOESY |
| 6 | 1 | 3 | 4D HCNH NOESY |
| 7 | 1 | 1 | 3D HNCO |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.5 | ambient | 297 |
Conformers
| Conformers Calculated Total Number | 100 |
| Conformers Submitted Total Number | 10 |
